Analytical Chemistry

Teacher

Bikash Samantaray

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Course Name: Analytical Chemistry

Course Code(Credit): CUTM2045(2-1-0)

Course Objectives

Understanding fundamental principles for environmental analytical methods.
To point out suitable analytical techniques for analyzing a specific compounds in an environmental matrix.

Course Outcomes

On completion of this course, the students will be able to gain knowledge on:

COs Course Outcomes Mapping COs with POs (High-3, Medium-2, Low-1)

CO1 To analyze chemical analysis and PO1(3)

laboratory work and its importance.

CO2 To plan and carryout laboratory experiments. PO2(3)

CO3 Gain knowledge on sampling and handling of PO3(2)

environmental s including data analysis samples.

Course Syllabus

Module-I

Water Analysis: Introduction to analytical chemistry and its application Lime-Soda, Zeolite and Ion exchange methods. Removal of DO and dissolvedCO2 from water by De-aeration method, Desalination of Brackish water by Reverse osmosis and electro dialysis process, Numerical on calculation of Temporary and Permanent hardness of water, Lime-Soda calculation

Practice

Determination of hardness of water by EDTA
Determination of alkalinity of water
Determination of Dissolved Oxygen in
Determination of Biological Oxygen
Determination of Chemical Oxygen

Module-II

Soil Analysis: Soil profile, Structure, and Soil properties, Determination of soil properties.

Practice

Determination of specific gravity of the soil by using
Determination of pH and electrical conductivity of soil
Determination of moisture content in soil by oven drying method.

Module-III

Fuel Analysis: Fuel, Classification of fuel, calorific value: gross and net calorific values, Determination of calorific value by bomb calorimeter, Proximate and ultimate analysis of coal and their importance, Numerical on calculation of calorific value and proximate and ultimate analysis of fuel.

Practice

Determination of calorific value of a fuel sample by using Bomb calorimeter

Module-IV

Petroleum: its chemical composition and fractional distillation, cracking of heavy oil residues – thermal and catalytic cracking, Knocking, Octane number, Synthesis and applications of bio- fuels, Photovoltaic cell.

Practice

Synthesis of bio diesel by transesterification process

Module-V

Electrochemical Phenomenon: Electrochemical cell, Electrode potential , Determination of pH of a solution Using Clomel/ Quin Hydrone Electrode, Corrosion-Mechanisms and its type, Factors affecting Corrosion; Protection from corrosion

Practice

Estimation of ferrous ion in the given solution using standard potassium dichromate.

Module-VI

Error in Chemical analysis: Types of errors, Accuracy and precision, Absolute and relative uncertainty, mean and standard deviation.

Text Books:

Engineering chemistry By Jain & Jain-16^th Edn,2015, Dhanpatrai publications
Engineering chemistry By Sashi Chawla,3^rd Edn, Dhanpatiroy publications,2011
Industrial Chemistry by K. Sharma 21^st Edn-2018, Satya Publications4.

Reference Books:

Applied Chemistry By Aruna Kumari-2^nd Edition, Paramount publications,2016
Engineering chemistry by OG Palanna, McGrahill Education(India) private Limited,2009
Engineering chemistry by K.Sesha Maheswaramma, Mridula. Chuch. Pearson India Education services pvt Ltd, 2016
EngineeringchemistrybyPrasanthRath,CengageLearningIndiapvtLtd,2013
V.Gadag,A.Nityananda,Shetty,I.K.InternationalPublishishing house,2006
Engineering chemistry –Fundamentals and applications, By Shika Agarwaal-Cambridge University Press Edition,2017