Analytical Techniques
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Analytical Techniques
Teacher
Chittaranjan Routray
Category
Core Courses
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Course Name : Analytical Techniques
Code(Credit) : CUTM1426(3-1-0)
Course Objectives
- To reinforce chemical principles central to analytical chemistry.
- To introduce instrumental techniques for chemical measurement.
- To develop critical thinking for interpreting analytical data.
- To select instrumentation appropriate to the measurement need.
- To gain an insight into the key methodologies used
Course Outcomes
| COs | Course outcomes | Mapping COs with POs (High-3, Medium-2, Low-1) |
| CO1 | Students will learn facts about major classes of instruments commonly used in chemical analysis. Their knowledge will be captured by the ability to block diagram these complex pieces of equipment, and tailor the specifications to the measurement needs. | PO1 (3) |
| CO2 | Analysts will develop the ability to apply calibration curves, internal standards and the method of standard addition as needed for various measurement problems. | PO2(3), PO4 (1) |
| CO3 | Able to Operate various analytical instruments | PO3(3), PO5(1), PO6(1) |
Course Syllabus
Module-1: Basic Tools of Analytical Methods
1.Chemical Measurements and Analytical tools
2.Experimental Error
3.Statistics and Quality Assurance
4.Chemical Equilibrium
5.Sample Preparation
Module-2: Chemical Equilibria for Quantitative Analysis-I
6.Gravimetric Analysis
7.Systematic Treatment
8.Monoprotic Acid-Base Equilibria
9.Polyprotic Acid-Base Equilibria
10.Acid-Base Titrations
11.Complexometric Titrations
Practise-1:Gravimetric Analysis of SULFATE as Barium Sulfate
Practise-2:Determination of the Concentration of Acetic Acid in its Commercial Solution (Vinegar)
Practise-3:Determination of the Concentration of Citric Acid in Commercial Soda
Practise-4:Determination of Number of Particles of Water Crystallization in Borax
Module-3: Electrochemical Analysis
12.Effects of Electrolytes
13.Fundamentals of Electrochemistry
14.Potentiometry and Conductometry
15.Redox Titrations
Module-4: Spectrophotometry
16.Fundamentals of Spectrophotometry
17.Applications of Spectrophotometry
18.Spectrophotometers
Module-5: Molecular analysis by Spectroscopy
19. Analysis by uv vis spectroscopy
20.Infrared Spectroscopy Analysis
21.NMR Spectroscopy analysis
Practise-5:Study of kinetics of a reaction by using spectrophotometric method
Module 6: Spectrochemical Analysis
22.Atomic absorption Spectroscopy
23.Mass Spectrometry
24.Vibrational spectroscopies
25.Electronic and optical sensors
Module-7: Analytical Separations
26. Introduction to Analytical Separations
27. Gas Chromatography
28. Liquid chromatography
29. High-Performance Liquid Chromatography
30. Electrophoresis Analyses
Practise-6:Separation of Amino Acids by Thin Layer Chromatography
Text Books
1. Instrumental Methods of analysis- Willard, Merrit, Dean and Settle.
2. Spectroscopic identification of organic compounds- R.M. Silverstein and G.C. Bassler
3. Spectroscopic methods in organic chemistry- D.H. Williams and I. Fleming
4. Absorption spectroscopy of organic molecules- V.M. Parikh
5. Applications of spectroscopic techniques in Organic chemistry- P.S. Kalsi
6. A Text book of Qualitative Inorganic Analysis- A. I. Vogel
7. Physical Methods in Inorganic Chemistry (DWAP)- R. Drago
8. Fundamentals of Analytical Chemistry – D.A. Skoog and D.M. West (Holt Rinehart and Winston Inc
Session Plan
Session 1
Chemical Measurements and Analytical tools
https://resources.saylor.org/wwwresources/archived/site/wp-content/uploads/2012/07/Chapter211.pdf
https://www.slideshare.net/NoeChan24/chapter-1-66059397
Session 3
Statistics and Quality Assurance
https://www.slideshare.net/SuchitraSahu/statistical-quality-control-presentation-77140537
Session 5
Practise-1:
Gravimetric Analysis of SULFATE as Barium Sulfate
http://vlab.amrita.edu/?sub=2&brch=193&sim=350&cnt=1
Session 7
Session 9
Monoprotic Acid-Base Equilibria
https://www.slideshare.net/CleophasRwemera/chapter-7-acids-and-bases
https://www.youtube.com/watch?v=qUHCuJ_DIrM
Session 10
Practise-2:
Determination of the Concentration of Acetic Acid in its Commercial Solution (Vinegar)
http://solr.bccampus.ca:8001/bcc/file/f5e15cfc-2799-be7f-16e4-1dc5cb67d77d/1/CHEM-Sem2-Lab4.zip/CHEM-Sem2-Lab8.pdf
https://www.youtube.com/watch?v=9pS7Q4MQCYI
Session 11
Polyprotic Acid-Base Equilibria
https://slideplayer.com/slide/6590969/
https://www.youtube.com/watch?v=Lrs707pdfXs
Session 13
Session 14
Effects of Electrolytes
https://www.youtube.com/watch?v=xhLHtuZ3VOI
https://www.youtube.com/watch?v=1p1cMFscF8s
Session 15
Fundamentals of Electrochemistry
https://www.slideserve.com/gaille/fundamentals-of-electrochemistry
https://www.youtube.com/watch?v=V5TqMuHaDuY
Session 17
Practise-3:
Determination of the Concentration of Citric Acid in Commercial Soda
http://classes.kvcc.edu/chm120/CitricAcid/CitricAcid.pdf
https://www.youtube.com/watch?v=q5Wp-0YxF8w
Session 18
Session 19
Fundamentals of Spectrophotometry
https://www.slideserve.com/drake/fundamentals-of-spectrophotometry
https://www.youtube.com/watch?v=qbCZbP6_j48
Session 20
Applications of Spectrophotometry
https://www.slideshare.net/rey216/spect
https://www.azom.com/article.aspx?ArticleID=10245
Session 21
Session 23
Practise-4:
Determination of Number of Particles of Water Crystallization in Borax
https://www.youtube.com/watch?v=F6GBT-dw3-M
Session 24
FT IR Techniques and applications
https://www.slideshare.net/GamalAbdulHamid/fourier-transform-infrared-spectroscopy-ftir
https://www.youtube.com/watch?v=Xw3Pk1jSNXQ
Session 25
Session 26
Session 27
Session 28
Vibrational spectroscopies
https://www.slideshare.net/cdtpv/vibrational-spectrroscopy
https://www.youtube.com/watch?v=3RqEIr8NtMI
Session 29
Electronic and optical sensors
https://slideplayer.com/slide/4716764/
https://www.youtube.com/watch?v=dxpZQjK2Gvk
https://www.youtube.com/watch?v=w8ml0Exihhc
Session 30
Practise-5:
Study of kinetics of a reaction by using spectrophotometric method
http://mas-iiith.vlabs.ac.in/exp10/simulation/exp10.html
Session 31
Introduction to Analytical Separations
https://slideplayer.com/slide/10636420/
https://www.youtube.com/watch?v=bUgFYdgKsqY
Session 32
Session 34
Session 36
Practise-6:
Separation of Amino Acids by Thin Layer Chromatography
http://vlab.amrita.edu/?sub=3&brch=63&sim=154&cnt=1
Case Studies
Case Studies
Our Main Teachers
Mr. Chittaranjan Routray, M.Sc ,Ph.D(Cont…) serving as Assistant Professor in the Department of Chemistry,School of Applied Sciences of Centurion University of Technology and Management, Odisha. He has more than 12 years of Experiences as an Academician as well as Researcher. His subject of expertise includes Polymer Chemistry, Spectroscopy, Nano Technology, Water Technology and Bio Chemistry […]