Applied Analytical Chemistry

Teacher

Dr. M.L.N Acharyulu

Category

Core Courses

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Course Name : Applied Analytical Chemistry

Code(Credit) : CUTM1008(2-1-0)

Course Objectives

  • To understand the in fundamental principles for  analytical methods (titration, electrochemistry, instrumentation) the  basic parameters of water, soil, fuel
  • To understand the applicability of  suitable analytical techniques for analyzing a specific components in Domestic,Agriculture,Commercial and Industrial samples

Course Outcomes

COs Course outcomes Mapping COs with POs (High-3, Medium-2, Low-1)
CO1 Able to gain Knowledge on various water softening methods, soil analysis methods, fuels, electrochemical phenomena and error analysis PO1 ( 3)
CO2 Analytical skill and Critical Thinking PO2(3), PO5(1)
CO3 Use of Tool, Design and Development (Hands-on/Technical skill) PO3(3)

Course Syllabus


Module-I (4Hrs)

Water softening processes: Lime-Soda, Zeolite and Ion exchange methods. Removal of DO and dissolved CO2 from water by De-aeration method,Desalination of Brackish water by Reverse osmosis and electro dialysis process,Numericals on calculation of Temporary and Permanent hardness of water,Lime-Soda calculation

Practice

1.Determination of hardness of water by EDTA method. (V. lab)
2.Determination of alkalinity of water. (V. lab)
3.Determination of Dissolved Oxygen in water. (V. lab)
4.Determination of Biological Oxygen Demand. (V. lab)
5.Determination of Chemical Oxygen Demand. (V. lab)

Module-II (2Hrs)
Soil Analysis: Soil profile, Structure, and properties, Determination of soil properties

Practice
6.Determination of specific gravity of the soil by using piknometer. (V.lab)
7.Determination of pH and electrical conductivity of soil sample.(V. lab)
8.Determination of moisture content in soil by oven drying method. (V. lab)

Module-III (3 Hrs)
Classification, combustion and chemical principles involved in fuel, calorific value: gross and net calorific values and their determination by bomb calorimeter , Proximate and ultimate analysis of coal and their importance. LPG, Water gas, producer gas, CNG .

Practice
9.Determination of calorific value of a fuel sample by using Bomb calorimeter.
10. Analysis of flue gases by Orsat’s apparatus.

Module-IV (4 Hrs)
Petroleum: its chemical composition and fractional distillation, cracking of heavy oil residues – thermal and catalytic cracking, knocking and chemical structure, octane number, synthesis and applications of bio-fuels, Photovoltaic cell.

Practice
11.Synthesis of biodiesel by trans esterification process

Module-V (3 Hrs)
Corrosion-Mechanisms, Factors affecting Corrosion; Protection from corrosion.

Practice
12.Estimation of ferrous ion in the given solution using standard potassium dichromate.

Module-VI (2Hrs)
Electrochemical Phenomenon
Electrochemical cell, Electrode potential, Determination of pH of a solution Using Clomel/ Quin Hydrone Electrode.

Module-VII (2Hrs)
Error in Chemical analysis
Types of errors, Accuracy and precision, Absolute and relative uncertainty, mean and standard deviation.

Text Books

  • Engineering chemistry By Jain &Jain-16th Edn,2015, Dhanpat rai publications
  • Engineering chemistry By Sashi Chawla,3rd Edn,Dhanpati roy publications,2011
  • Industrial Chemistry By B.K.Sharma 21 st Edn-2018,Satya Publications4.

Reference Books

  • Applied Chemistry By Aruna Kumari-2nd Edition,Paramount publications,2016
  • Engineering chemistry by OG Palanna,McGrahill Education(India) private Limited,2009
  • Engineering chemistry by K.Sesha Maheswaramma,Mridula.Chuch.PearsonIndia Education services pvt Ltd,2016
  • Engineering chemistry by Prasanth Rath,Cengage Learning India pvtLtd,2013
  • Engineering chemistry by R.V.Gadag,A.Nityananda, Shetty,I.K.International Publishishing house,2006
  • Engineering chemistry –Fundamentals and applications,ByShika Agarwaal-Cambridge University PressEdition,2017

Session 7

Soil Analysis: Soil profile, Structure, and properties, Determination of soil properties

https://nptel.ac.in/content/syllabus_pdf/105101005
https://www.nrcs.usda.gov/wps/portal/nrcs/detail/

Session 10

Classification, combustion and chemical principles involved in fuel

https://www.slideshare.net/pradyumnagujjar7/fuels-33032404

Session 12

Session 13

LPG, Water gas, producer gas, CNG.

Session 14

Determination of calorific value of a fuel sample by using Bomb calorimeter
Analysis of flue gases by Orsat’s apparatus

Session 18

Synthesis of biodiesel by transesterification process

Session 19

Session 22

Determination of ferrous ion in the given solution using standard potassium dichromate

Session 24

Determination of pH of a solution Using Clomel/ Quin Hydrone Electrode.

https://www.youtube.com/watch?v=naYbESrjylI

Session 25

Types of errors, Accuracy and precision, Absolute and relative uncertainty

https://www.youtube.com/watch?v=fk4_t-csbbgslideshare.net/mrjdfield/calculating-uncertainties-30710692

Case Studies

Our Main Teachers

Dr. M.L.N Acharyulu

Associate Professor Chemistry, H.O.D (Basic Sciences and Humanities ) ,Associate Dean (SPAHS)
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Commited to the Feild Of Teaching for the past 25 years. Experienced in Presentation skills , Published 25 Journals and 14 Papers in National and International Journals.