Analytical Techniques

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Analytical Techniques

Analytical Techniques


Chittaranjan Routray


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Course Name : Analytical Techniques

Code(Credit) : CUTM1426(3-1-0)

Course Objectives

  • To reinforce chemical principles central to analytical chemistry.
  • To introduce instrumental techniques for chemical measurement.
  • To develop critical thinking for interpreting analytical data.
  • To select instrumentation appropriate to the measurement need.
  • To gain an insight into the key methodologies used

Course Outcomes

COs Course outcomes Mapping COs with POs (High-3, Medium-2, Low-1)
CO1 Students will learn facts about major classes of instruments commonly used in chemical analysis. Their knowledge will be captured by the ability to block diagram these complex pieces of equipment, and tailor the specifications to the measurement needs. PO1 (3)
CO2 Analysts will develop the ability to apply calibration curves, internal standards and the method of standard addition as needed for various measurement problems. PO2(3), PO4 (1)
CO3 Able to Operate various analytical instruments PO3(3), PO5(1), PO6(1)

Course Syllabus

Module-1: Basic Tools of Analytical Methods
1.Chemical Measurements and Analytical tools
2.Experimental Error
3.Statistics and Quality Assurance
4.Chemical Equilibrium
5.Sample Preparation

Module-2: Chemical Equilibria for Quantitative Analysis-I
6.Gravimetric Analysis
7.Systematic Treatment
8.Monoprotic Acid-Base Equilibria
9.Polyprotic Acid-Base Equilibria
10.Acid-Base Titrations
11.Complexometric Titrations

Practise-1:Gravimetric Analysis of SULFATE as Barium Sulfate
Practise-2:Determination of the Concentration of Acetic Acid in its Commercial Solution (Vinegar)
Practise-3:Determination of the Concentration of Citric Acid in Commercial Soda
Practise-4:Determination of Number of Particles of Water Crystallization in Borax

Module-3: Electrochemical Analysis
12.Effects of Electrolytes
13.Fundamentals of Electrochemistry
14.Potentiometry and Conductometry
15.Redox Titrations

Module-4: Spectrophotometry
16.Fundamentals of Spectrophotometry
17.Applications of Spectrophotometry

Module-5: Molecular analysis by Spectroscopy
19. Analysis by uv vis spectroscopy
20.Infrared Spectroscopy Analysis
21.NMR Spectroscopy analysis

Practise-5:Study of kinetics of a reaction by using spectrophotometric method

Module 6: Spectrochemical Analysis
22.Atomic absorption Spectroscopy
23.Mass Spectrometry
24.Vibrational spectroscopies
25.Electronic and optical sensors

Module-7: Analytical Separations

26. Introduction to Analytical Separations
27. Gas Chromatography
28. Liquid chromatography
29. High-Performance Liquid Chromatography
30. Electrophoresis Analyses

Practise-6:Separation of Amino Acids by Thin Layer Chromatography

Text Books
1. Instrumental Methods of analysis- Willard, Merrit, Dean and Settle.
2. Spectroscopic identification of organic compounds- R.M. Silverstein and G.C. Bassler
3. Spectroscopic methods in organic chemistry- D.H. Williams and I. Fleming
4. Absorption spectroscopy of organic molecules- V.M. Parikh
5. Applications of spectroscopic techniques in Organic chemistry- P.S. Kalsi
6. A Text book of Qualitative Inorganic Analysis- A. I. Vogel
7. Physical Methods in Inorganic Chemistry (DWAP)- R. Drago
8. Fundamentals of Analytical Chemistry – D.A. Skoog and D.M. West (Holt Rinehart and Winston Inc


Session 5

Gravimetric Analysis of SULFATE as Barium Sulfate

Session 10

Session 17

Determination of the Concentration of Citric Acid in Commercial Soda

Session 30

Study of kinetics of a reaction by using spectrophotometric method

Session 36

Separation of Amino Acids by Thin Layer Chromatography

Case Studies

Case Studies

Our Main Teachers

Mr. Chittaranjan Routray, M.Sc ,Ph.D(Cont…) serving as Assistant Professor in the Department of Chemistry,School of Applied Sciences of Centurion University of Technology and Management, Odisha. He has more than 12 years of Experiences as an Academician as well as Researcher.  His subject of expertise includes Polymer Chemistry, Spectroscopy, Nano Technology, Water Technology and Bio Chemistry […]