PHARMACEUTICAL ANALYSIS-I (PRACTICAL)

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Satyanarayan Tripathy

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Course Name : PHARMACEUTICAL ANALYSIS-I (PRACTICAL)

Code(Credit) : BPHL1102 (0-2-0)

Course Objectives

Know the fundamentals of analytical chemistry
principles of electrochemical analysis of drugs
Principle of volumetric and electrochemical titrations
Objective of standardization and validation

Course Outcomes

CO	Statements	Mapping With POs
CO1	*define, express* and analyze the qualitative and quantitative estimation of Pharmaceuticals, the units of concentration and the problems related to it.	PO1, PO2, PO3, PO11
CO2	*describe, explain* and *apply* the different concepts of acid-base titration & the different assay procedures.	PO1, PO2, PO3, PO11
CO3	*describe, analyze* and *apply* the principle of Precipitation titration in Mohr’s, Volhard’s and Fajan’s Method, also able to *explain* the principle of gravimetry and diazotization titration.	PO1, PO3, PO2, PO11
CO4	*define and distinguish* different types of reductant, oxidant and also able to *explain* different types of redox reaction.	PO1, PO2, PO3, PO11
CO5	*explain* and *apply* different types of electrochemical methods of analysis.	PO1, PO2, PO4, PO11

Course Syllabus

MODULE -I Limit Test of the following

(1) Chloride (2) Sulphate (3) Iron (4) Arsenic

MODULE - II Preparation and standardization of

(1) Sodium hydroxide (2) Sulphuric acid (3) Sodium thiosulfate (4) Potassium permanganate (5) Ceric ammonium sulphate

MODULE - III Assay of the following compounds along with Standardization of Titrant

(1) Ammonium chloride by acid base titration (2) Calcium gluconate by complexometry (3) Sodium benzoate by non-aqueous titration (4) Sodium Chloride by precipitation titration

MODULE- IV Preparation and standardization of

(1) Ceric ammonium sulphate (2) KMNO4

MODULE -V Determination of Normality by electro-analytical methods

(1) Conductometric titration of strong acid against strong base (2) Conductometric titration of strong acid and weak acid against strong base (3) Potentiometric titration of strong acid against strong base

BOOK REFERENCES